Thionyl Chloride → HCID 19068257, compound

Participants

Reaction Steps

1.78 g (5 mmol) of 3-(1-adamantyl)-4-methoxycarbonylmethyloxybenzoic acid and 15 ml of thionyl chloride were introduced into a round-bottomed flask and the mixture was heated at reflux for one hour. It was evaporated to dryness and the crude acid chloride, which was used without further purification in the remainder of the synthesis, was recovered.

Provenance & Evidence