HRID1957974

反应详情

EQUATION

反应方程式

HRID 1957974 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

1-(Ethylsulfonyl)-3-nitro-benzene (1.9 g; 9 mmol) was dissolved in 80 mL of methanol then 1 g of Raney-Nickel is added and the mixture treated with hydrogen gas. The reaction mixture was subsequently filtered and concentrated to yield 1.5 g (8.1 mmol; yield=93%) of an yellow oil.

WORKUP

后处理

  1. filtrationThe reaction mixture was subsequently filtered
  2. concentrationconcentrated
  3. customto yield 1.5 g (8.1 mmol; yield=93%) of an yellow oil