HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Ethanesulfonyl-3-nitro-benzene → 3-(Ethanesulfonyl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Ethanesulfonyl-3-nitro-benzene | HCID 12744585 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-(Ethanesulfonyl)aniline | HCID 12744595 | — |
Reaction Steps
1-(Ethylsulfonyl)-3-nitro-benzene (1.9 g; 9 mmol) was dissolved in 80 mL of methanol then 1 g of Raney-Nickel is added and the mixture treated with hydrogen gas. The reaction mixture was subsequently filtered and concentrated to yield 1.5 g (8.1 mmol; yield=93%) of an yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410100B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-42afc673a9f24bb9acaa16317ba32abb |
| Source note | uspto-grants-2013_04 |