HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-chloro-8-isopropyl-5-methyl-7,8-dihydro-5H-pteridin-6-one → HCID 68422327, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-chloro-8-isopropyl-5-methyl-7,8-dihydro-5H-pteridin-6-one | HCID 58405900 | — |
| Reactant | 3-(Methanesulfonyl)-5-nitroaniline | HCID 67359315 | — |
| Product | HCID 68422327 | HCID 68422327 | 58.1% |
Reaction Steps
Starting from 2-chloro-8-isopropyl-5-methyl-7,8-dihydro-5H-pteridin-6-one (9.35 g; 38.85 mmol) and 3-methansulfonyl-5-nitro-phenylamine (8.4 g; 38.5 mmol), 9.4 g (22.38 mmol; 57.5% yield) of the desired nitro-product were obtained as a powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410100B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-979050b490d448e4ad5508f08ab8bb99 |
| Source note | uspto-grants-2013_04 |