HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol, 2-[(3-aminophenyl)sulfonyl]- → HCID 59286160, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol, 2-[(3-aminophenyl)sulfonyl]- | HCID 78905 | — |
| Reactant | 2-chloro-8-isopropyl-5-methyl-7,8-dihydro-5H-pteridin-6-one | HCID 58405900 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59286160 | HCID 59286160 | 85% |
Reaction Steps
2-Chloro-8-isopropyl-5-methyl-7,8-dihydro-5H-pteridin-6-one (150 mg; 0.623 mmol) and 2-(3-Amino-phenylsulfonyl)-ethanol (120 mg; 0.600 mmol) were heated to 160° C. for 30 minutes. The reaction mixture was then suspended in dichloromethane and ethyl acetate then filtrated to yield 215 mg (0.530 mmol; 85% yield) as yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410100B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-e6f8360d980f4d35beeed0dc9faad072 |
| Source note | uspto-grants-2013_04 |