Hydrochloric Acid → HCID 58367580, compound

HRID 1958697Notes

Reaction equation

HRID 1958697 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[S:12][C:11]([C:13]([N:15]2[CH2:20][CH2:19][C:18]([C:24]3[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=3)([C:21]([NH2:23])=[O:22])[CH2:17][CH2:16]2)=[O:14])=[CH:10][C:9]=1[C:30]1[CH:35]=[CH:34][C:33]([O:36][CH2:37][CH2:38][CH2:39][O:40]C2CCCCO2)=[CH:32][CH:31]=1.Cl>CO>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[S:12][C:11]([C:13]([N:15]2[CH2:20][CH2:19][C:18]([C:24]3[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=3)([C:21]([NH2:23])=[O:22])[CH2:17][CH2:16]2)=[O:14])=[CH:10][C:9]=1[C:30]1[CH:35]=[CH:34][C:33]([O:36][CH2:37][CH2:38][CH2:39][OH:40])=[CH:32][CH:31]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 67184184HCID 67184184, compound

Product 1

HCID 58367580HCID 58367580, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

0.45 g of the compound obtained in stage 23H) and 2 ml of 2N ethereal hydrochloric acid are added to 10 ml of methanol. After 2 hours at AT, the expected compound is filtered off 0.26 g of the expected compound is obtained.

Workup

  1. filtrationthe expected compound is filtered off 0.26 g of the expected compound
  2. customis obtained

Sources & evidence

ORD record
ord-00f10fe04a33419594ea88e2e848ec84
Source dataset
uspto-grants-2013_04
Patent number
US08410137B2

Reaction notes

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