HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 68742763, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 86641230 | HCID 86641230 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68742763 | HCID 68742763 | — |
Reaction Steps
To a solution of (R)-benzyl 4-(dimethylamino)-3-(5-(m-tolylethynyl)thiophene-2-sulfonamido)butanoate (25 mg, 0.05 mmol) and methyl iodide (100 μL, 40 eq) in CH2Cl2 (1 mL) was stirred overnight at room temperature. The solution was concentrated to give the title compound in quantitative yield. MS ESI 511.3 [M]+, calcd for [C27H31N2O4S2]+ 511.17.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410150B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-1a3df8f58818401ab0095ecc445cf7cf |
| Source note | uspto-grants-2013_04 |