HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Ethynyl-4-pentylbenzene → HCID 86641233, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Ethynyl-4-pentylbenzene | HCID 2775131 | — |
| Reactant | HCID 59294388 | HCID 59294388 | — |
| Product | HCID 86641233 | HCID 86641233 | 91% |
Reaction Steps
According to the method described in example S76a, (R)-benzyl 3-(5-bromothiophene-2-sulfonamido)-4-(dimethylamino)butanoate was reacted with 1-ethynyl-4-pentylbenzene to give the title compound as a black oil (68 mg, 91%). MS ESI 553.3 [M+H]+, calcd for [C30H36N2O4S2+H]+ 553.21.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410150B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-f89de32672f142e4bfcf1c7f1125ee71 |
| Source note | uspto-grants-2013_04 |