HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxy-2-Methoxybenzaldehyde → 4-Hydroxy-2-methoxybenzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxy-2-Methoxybenzaldehyde | HCID 519541 | — |
| Reactant | 3-Ethyl-4-hydroxy-5-methylbenzonitrile | HCID 59759950 | — |
| Product | 4-Hydroxy-2-methoxybenzonitrile | HCID 10953681 | — |
Reaction Steps
The title compound is prepared from commercially available 4-hydroxy-2-methoxy-benzaldehyde in analogy to literature procedures (see 3-ethyl-4-hydroxy-5-methyl-benzonitrile). LC-MS: tR=0.74 min. 1H NMR (D6-DMSO): δ 3.84 (s, 3H), 6.47 (d, J=8.5 Hz, 1H), 6.54 (s, 1H), 7.49 (d, J=8.5 Hz, 1H), 10.60 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410151B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-619069db00df41d19ee8f2935423468c |
| Source note | uspto-grants-2013_04 |