HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxy-2-Methoxybenzaldehyde → HCID 178493425, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxy-2-Methoxybenzaldehyde | HCID 519541 | — |
| Reactant | HCID 178436626 | HCID 178436626 | — |
| Product | HCID 178493425 | HCID 178493425 | — |
Reaction Steps
The title compound is prepared from commercially available 4-hydroxy-2-methoxybenzaldehyde in analogy to literature procedures (see 3-ethyl-4,N-dihydroxy-5-methyl-benzamidine). LC-MS: tR=0.41 min; [M+1]+=183.06; 1H NMR (D6-DMSO): δ 3.74 (s, 3H), 5.47 (s, 2H), 6.35 (dd, J=8.3, 1.5 Hz, 1H), 6.45 (s, 1H), 7.21 (d, J=8.5 Hz, 1H), 9.42 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410151B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-8848b084b4564a4a8e3f75b38b9890c2 |
| Source note | uspto-grants-2013_04 |