Carbon Tetrachloride → HCID 67078081, compound

Participants

Reaction Steps

Polymer bound triphenylphosphine (3 mmol/g, 234 mg, 0.702 mmol) and CCl4 (400 μL) were added to a stirred solution of 5-chloro-4-hydroxymethyl-nicotinic acid methyl ester (14.2 mg, 0.070 mmol) in DCM (4 mL). After stirring for 2 h at room temperature, the reaction mixture was filtered and concentrated in vacuo. The resulting title compound was used for the next reaction without purification. MS (m/z): 220.1 [M+H+].

Provenance & Evidence