HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1959584Generated: November 4, 2026
Potassium tert-butoxide → HCID 44190365, compound
https://huagongshe.com/reaction/1959584
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Reactant | HCID 44190364 | HCID 44190364 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 44190365 | HCID 44190365 | — |
Reaction Steps
Potassium tert-butylate (1.77 g, 15.80 mmol) was added to a stirred solution of 3,5-dichloro-4-(tetrahydro-pyran-2-yloxymethyl)-pyridine (825 mg, 3.16 mmol) in dioxane. After stirring for 3 d at 100° C. the solvent was removed in vacuo. The resulting title compound was used for the next reaction without purification. MS (m/z): 243.8 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08410134B2 |
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| Source dataset | uspto-grants-2013_04 |
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| ORD ID | ord-ab3b9aa7343b42c289b5cedf45898f18 |
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| Source note | uspto-grants-2013_04 |
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