HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 67078322, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 67077290 | HCID 67077290 | — |
| Reactant | HCID 67077751 | HCID 67077751 | — |
| Product | HCID 67078322 | HCID 67078322 | — |
Reaction Steps
[3-Chloro-5-(tetrahydro-pyran-2-ylmethoxy)-pyridin-4-yl]-methanol (10 mg, 0.039 mmol) was chlorinated with SOCl2 according to the synthesis of 3-(1-butyl-1H-imidazol-2-ylsulfanyl)-5-chloro-4-chloromethyl-pyridine. The resulting title compound was used for the next reaction without purification. MS (m/z): 276.0 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410134B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-92dea9784ded4450ace6d5e7114a15f7 |
| Source note | uspto-grants-2013_04 |