HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 67077180, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3,5-Dichloro-4-(chloromethyl)pyridine | HCID 22626853 | — |
| Reactant | HCID 67078189 | HCID 67078189 | — |
| Product | HCID 67077180 | HCID 67077180 | — |
Reaction Steps
N-(5-Chloro-4-hydroxymethyl-pyridin-3-ylmethyl)-3-methyl-succinamic acid methyl ester (1.39 mg, 0.0046 mmol) was chlorinated with SOCl2 according to the synthesis of 3,5-dichloro-4-chloromethyl-pyridine. The resulting title compound was used for the next reaction without purification. MS (m/z): 318.9 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410134B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-32a3f8a7e04a41019bb593d5943c5918 |
| Source note | uspto-grants-2013_04 |