HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1959598Generated: November 2, 2026
4-Chloro-8-hydroxy-2-methylquinoline → HCID 67077596, compound
https://huagongshe.com/reaction/1959598
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Chloro-8-hydroxy-2-methylquinoline | HCID 12219722 | — |
| Reactant | HCID 178434161 | HCID 178434161 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67077596 | HCID 67077596 | — |
Reaction Steps
A mixture of 4-chloro-2-methyl-quinolin-8-ol (10 mg, 52 μmol) and 5-methyl-[1,3,4]thiadiazole-2-thiol (6.9 mg, 52 μmol) in MeOH (0.3 mL) was heated to 80° C. for 1.5 h. The solvent was removed in vacuo to give title compound. MS (m/z): 289.9 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08410134B2 |
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| Source dataset | uspto-grants-2013_04 |
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| ORD ID | ord-35cdf1bf3c1b4e08889535c8baa0d4f8 |
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| Source note | uspto-grants-2013_04 |
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