HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloropyridine-3-carbaldehyde → HCID 86645362, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloropyridine-3-carbaldehyde | HCID 15053985 | — |
| Reactant | (3,5-Dichloropyridin-4-yl)methanol | HCID 17855219 | — |
| Reactant | HCID 44190473 | HCID 44190473 | — |
| Reactant | 2,4-Dichloropyridine-3-methanol | HCID 53393177 | — |
| Product | HCID 86645362 | HCID 86645362 | — |
Reaction Steps
2,4-Dichloro-pyridine-3-carbaldehyde (1.565 g. 8.89 mmol) was reduced to (2,4-dichloro-pyridin-3-yl)-methanol according to the procedure described for the preparation of (3,5-dichloro-pyridin-4-yl)-methanol and subsequently protected with the THP-group according to the procedure described for the preparation 3-bromo-5-chloro-4-(tetrahydro-pyran-2-yloxymethyl)-pyridine to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410134B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-746704c4ce17408997a6792fbe7a5bfc |
| Source note | uspto-grants-2013_04 |