HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → O-Benzylhydroxylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | N-Benzyloxyphthalimide | HCID 255292 | — |
| Product | O-Benzylhydroxylamine | HCID 102313 | 64% |
Reaction Steps
The title compound was prepared from 2-(benzyloxy)isoindoline-1,3-dione and hydrazine monohydrate in 64% yield using the same procedure as described in the synthesis of intermediate G. 1H-NMR (400 MHz, CDCl3) δ ppm 7.37 (m, 5H), 6.70 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410264B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-f1a1c170837c4e9391e84901aa090197 |
| Source note | uspto-grants-2013_04 |