HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenol → HCID 86661968, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenol | HCID 2734624 | — |
| Reactant | Diethyl P-[[[(4-methylphenyl)sulfonyl]oxy]methyl]phosphonate | HCID 4193599 | — |
| Product | HCID 86661968 | HCID 86661968 | 23% |
Reaction Steps
Using 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol (313 mg, 1.42 mmol) and (diethoxyphosphoryl)methyl 4-methylbenzenesulfonate (550 mg, 1.71 mmol), the desired title compound (121 mg, yield 23%) was obtained by the same method as in Reference Example 2 (2a).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410273B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-305b50eea2ec4efd9c29e474145952a7 |
| Source note | uspto-grants-2013_04 |