HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydro-4H-pyran-4-ol → HCID 66730471, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydro-4H-pyran-4-ol | HCID 74956 | — |
| Reactant | HCID 14004864 | HCID 14004864 | — |
| Product | HCID 66730471 | HCID 66730471 | 85.3% |
Reaction Steps
Using tetrahydro-4-pyranol (0.784 mL, 8.23 mmol) and 2-[2-(benzyloxy)ethoxy]ethyl 4-methylbenzenesulfonate (1.92 g, 5.48 mmol) synthesized in Reference Example 6 (6a), the desired title compound (1.31 g, yield 85%) was obtained by the same method as in Reference Example 2 (2a).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410273B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-a30f792e4860403ca0941869ad4b750f |
| Source note | uspto-grants-2013_04 |