HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylethanediol → 2-[4-(2-Isopropoxyethoxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylethanediol | HCID 7996 | — |
| Reactant | 4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenol | HCID 2734624 | — |
| Product | 2-[4-(2-Isopropoxyethoxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane | HCID 66730421 | 31% |
Reaction Steps
Using 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol (609 mg, 2.76 mmol) and ethylene glycol monoisopropyl ether (432 mg, 4.15 mmol), the desired title compound (100 mg, yield 31%) was obtained by the same method as in Example 2 (2a).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410273B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-a6d68013bf914849ae53afb8952dbd53 |
| Source note | uspto-grants-2013_04 |