HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 66730432, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 66730412 | HCID 66730412 | — |
| Product | HCID 66730432 | HCID 66730432 | 83% |
Reaction Steps
Using 4-[2-(tetrahydro-2H-pyran-2-yloxy)ethoxy]piperidine (561 mg, 2.54 mmol) synthesized in (17b) and methanesulfonyl chloride (375 μL, 3.06 mmol), the desired title compound (618 mg, yield 83%) was obtained by the same method as in Reference Example 2 (2c).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08410273B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-b2ad346d830543daa717365df00236f4 |
| Source note | uspto-grants-2013_04 |