HRID19612

反应详情

EQUATION

反应方程式

HRID 19612 的结构方程式

PROCEDURE

实验过程

To a solution of 5-(4-iodo-phenyl)-7-methylsulfanyl-pyrazolo[1,5-c]pyrimidin (1000 mg) in chlorobenzene N-bromosuccinimide (730 mg) is added. The mixture is stirred for 1 hour then the chlorobenzene is evaporated. The residue is partitioned between ethylacetate and sodium-hydrogencarbonate (5%).

WORKUP

后处理

  1. customthe chlorobenzene is evaporated
  2. customThe residue is partitioned between ethylacetate and sodium-hydrogencarbonate (5%)