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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1961424Generated: November 1, 2026

HCID 57289411, compound → HCID 582382, compound

https://huagongshe.com/reaction/1961424

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57289411HCID 57289411—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 582382HCID 582382—

Reaction Steps

4-Cyclohexenylbenzonitrile (404 mg, 2.2 mmol) was dissolved in 15 ml EtOH and 40 mg 10% Pd/C was added. The reaction mixture was stirred under H2 at 3.0 atm. over night at room temperature. The mixture was filtered through celite with EtOAc washing. The filtrate was concentrated and the crude product 350 mg (86%) was used directly in the next step.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08415333B2
Source datasetuspto-grants-2013_04
ORD IDord-869b93e70902403dac3b09cc5d24e630
Source noteuspto-grants-2013_04