HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57289411, compound → HCID 582382, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57289411 | HCID 57289411 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 582382 | HCID 582382 | — |
Reaction Steps
4-Cyclohexenylbenzonitrile (404 mg, 2.2 mmol) was dissolved in 15 ml EtOH and 40 mg 10% Pd/C was added. The reaction mixture was stirred under H2 at 3.0 atm. over night at room temperature. The mixture was filtered through celite with EtOAc washing. The filtrate was concentrated and the crude product 350 mg (86%) was used directly in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08415333B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-869b93e70902403dac3b09cc5d24e630 |
| Source note | uspto-grants-2013_04 |