HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66632804, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 68089767 | HCID 68089767 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 66632804 | HCID 66632804 | — |
Reaction Steps
tert-Butyl 3-cyano-4-(4,4-dimethylpiperidin-1-yl)benzylcarbamate (250 mg, 0.73 mmol) was dissolved in Et2O (10 ml). HCl (2.0 M in Et2O)(10 ml) was added to the solution. The mixture was stirred for 36 h. The solvents were removed and the residue was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08415333B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-f24237b36fa546fab5e0a32f534f374b |
| Source note | uspto-grants-2013_04 |