反应详情

tert-Butyl 4-azido-3-iodobenzylcarbamate (936.0 mg, 2.5 mmol) was dissolved in Et2O.HCl (2.0 N in Et2O) (10 ml) was added to the solution. The mixture was stirred at r.t. overnight. The solvent was removed under vacuum and the residue washed with a mixture of CH2Cl2 and MeOH (8:2) affording 350 mg (45%) of the title compound.

1. additionwas added to the solution
2. customThe solvent was removed under vacuum
3. washthe residue washed with a mixture of CH2Cl2 and MeOH (8:2)