HRID1961490

反应详情

EQUATION

反应方程式

HRID 1961490 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

CONDITIONS

反应条件

温度
85 °C

PROCEDURE

实验过程

N-(4-tert-Butyl-2-hydroxybenzyl)-2-chloroacetamide (270.0 mg, 1.06 mmol) was dissolved in a mixture of EtOH (4.0 ml) and conc. HCl (1.3 ml). The mixture was stirred at 85° C. for 3.0 h. The solvents were removed under vacuum to afford 225 mg (98%) of the title compound.

WORKUP

后处理

  1. customThe solvents were removed under vacuum