HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzenesulfonyl Chloride → HCID 57989836, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzenesulfonyl Chloride | HCID 2734258 | — |
| Reactant | HCID 57989889 | HCID 57989889 | — |
| Product | HCID 57989836 | HCID 57989836 | — |
Reaction Steps
Following a procedure analogous to the procedure described in Intermediate 14 using 3-[2-(1,1-dimethylethyl)-5-(4-pyrimidinyl)-1,3-thiazol-4-yl]-2-fluoroaniline (70 mg, 0.213 mmol) and 3-fluorobenzenesulfonyl chloride (124 mg, 0.639 mmol), the title compound was obtained as a solid (76 mg, 73% yield). MS (ESI): 488 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08415345B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-fd3b4f5b376040ffabbd5e7c5c97e5e2 |
| Source note | uspto-grants-2013_04 |