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HRID1962892

反应详情

EQUATION

反应方程式

HRID 1962892 的结构方程式

REACTANTS

反应物

2
结构：O=P(Cl)(Cl)Cl
HCID24813

Phosphoric trichloride

Cl3OP

结构：O=c1nc(-c2ccc(C(F)(F)F)nc2)cc(C(F)(F)F)[nH]1
HCID87383493

未命名化合物

PRODUCTS

生成物

1
结构：FC(F)(F)c1ccc(-c2cc(C(F)(F)F)nc(Cl)n2)cn1
HCID86624628

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(6-trifluoromethyl-pyridin-3-yl)-6-trifluoromethyl-1H-pyrimidin-2-one (6.87 g, 0.022 mol) and phosphoroxychloride (35 ml) according to the general procedure I. Obtained as a light brown solid (7.18 g, 99%). MS (ISP) 329.2 [(M+H)+]; mp 87° C.