HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium periodate → HCID 66732355, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium periodate | HCID 23667635 | — |
| Reactant | 1-Piperidinecarboxylic acid, 2-(2,2-dimethylpropyl)-4-(hydroxymethyl)-, methyl ester | HCID 66731661 | — |
| Catalyst | Ruthenium trichloride | HCID 61850 | — |
| Product | HCID 66732355 | HCID 66732355 | — |
Reaction Steps
The compound was prepared as described in Reference Compound 4, Step 5 starting from methyl 4-(hydroxymethyl)-2-neopentylpiperidine-1-carboxylate, sodium periodate (15.0 g, 70.3 mmol) and ruthenium(III) chloride (0.11 g, 0.52 mmol), which resulted in the title compound. MS m/z 256 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08415378B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-b1b778c6b2f6451091e4e9eb38f4beb4 |
| Source note | uspto-grants-2013_04 |