HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium periodate → HCID 66732333, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium periodate | HCID 23667635 | — |
| Reactant | HCID 66732283 | HCID 66732283 | — |
| Catalyst | Ruthenium trichloride | HCID 61850 | — |
| Product | HCID 66732333 | HCID 66732333 | 87% |
Reaction Steps
The compound was prepared as described in Reference Compound 4, Step 5 starting from methyl 4-(hydroxymethyl)-2-(2-methyl-2-phenylpropyl)piperidine-1-carboxylate (8.0 g, 26.2 mmol), sodium periodate (16.8 g, 78.6 mmol) and ruthenium(III) chloride (0.12 g, 0.58 mmol), which resulted in the title compound (7.24 g, 87%). MS m/z 318 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08415378B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-e7b8a5504c08408ca998b289f8c9fd14 |
| Source note | uspto-grants-2013_04 |