HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86627028, compound → HCID 57572455, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86627028 | HCID 86627028 | — |
| Solvent | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 57572455 | HCID 57572455 | — |
Reaction Steps
The title compound was prepared from the product of step (iii) (0.6 g) which was stirred in TFA/DCM (1:1, 10 ml) overnight. The mixture was concentrated under reduced pressure to give an oil. The residue was purified by reverse phase HPLC, yield 0.31 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08415394B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-c7661fd39e314245a982ed2ca6543da6 |
| Source note | uspto-grants-2013_04 |