HRID19645

反应详情

EQUATION

反应方程式

HRID 19645 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 1-(3,3-dimethyl-6-nitroindolin-1-yl)ethanone (300 mg), 10% Pd—C (50 mg), and EtOH (50 mL) was stirred under hydrogen atmosphere (1 atm) for 3 h. The catalyst was filtered out and the filtrate was concentrated to give a light yellow solid (260 mg).

WORKUP

后处理

  1. filtrationThe catalyst was filtered out
  2. concentrationthe filtrate was concentrated