HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21081086, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21081084 | HCID 21081084 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21081086 | HCID 21081086 | — |
Reaction Steps
13 g of 3-[4-(acetylamino-methyl)-cyclohexyl]-propionic acid are added to 200 ml of semi-concentrated aqueous hydrochloric acid and the resulting solution is refluxed overnight. The mixture is combined with acetone, recrystallised and the precipitate is separated off. When the mother liquor is concentrated step by step further fractions of the crystallin product are isolated. The fractions are combined, recrystallised with isopropanol and then dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08420630B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-3f685ec3784541c3a95290ada173894c |
| Source note | uspto-grants-2013_04 |