HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66657281, compound → HCID 66657263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66657281 | HCID 66657281 | — |
| Solvent | Ethanol hydrochloride | HCID 21887872 | — |
| Product | HCID 66657263 | HCID 66657263 | 272% |
Reaction Steps
3(S)-[(3,4-dichlorophenyl)phenylamino]pyrrolidine-1-carboxylic acid tert-butyl ester (0.13 g) was dissolved in 1 N hydrochloric acid-ethanol and heated under reflux for one hour. The reaction solution was concentrated to dryness to thereby obtain 0.11 g of brown amorphous solid 3(S)-(3,4-dichlorophenyl)phenylpyrrolidin-3-ylamine hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08420623B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-5e07a6b473ae4f55976908bbc4cc3d15 |
| Source note | uspto-grants-2013_04 |