HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 6419992, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Riluzole | HCID 5070 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 6419992 | HCID 6419992 | — |
Reaction Steps
To a solution of 2-amino-6-(trifluoromethoxy)-benzothiazole in methanol (10 ml) is added 37% HCl (1 ml) dropwise, and the precipitate recrystallised from methanol to give quantitative yield of the hydrochloride, as white needles, m.p.: 214-216° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08420634B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-1d33b85f8432421fbc1bc863b9216d78 |
| Source note | uspto-grants-2013_04 |