HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 5-Hexenimidamide hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Methyl 5-hexenimidoate hydrochloride | HCID 86630239 | — |
| Product | 5-Hexenimidamide hydrochloride | HCID 55284960 | — |
Reaction Steps
Methyl 5-hexenimidoate hydrochloride (P3, 1.5 g) was dissolved in NH3 (2M in MeOH, 46 mL) and the mixture was heated to reflux for 2 h. Volatiles were evaporated in vacuo to give 1.45 g of the title compound as brown solid, which was used in the subsequent step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07745458B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-eed303558d374f6ab84a1de5e6dcf6e0 |
| Source note | uspto-grants-2010_06 |