HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenemethanamine, 3,4-dichloro- → HCID 59474745, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenemethanamine, 3,4-dichloro- | HCID 1608 | — |
| Reactant | HCID 43668467 | HCID 43668467 | — |
| Catalyst | Cupric sulfate monohydrate | HCID 61499 | — |
| Product | HCID 59474745 | HCID 59474745 | — |
Reaction Steps
Preparation was made using a similar procedure as described in example 5, method 5.1. Starting materials were 4-chloro-2-methyl-8-propoxyquinoline and 3,4-dichlorobenzylamine. A catalytic effective amount of copper(II)sulphate hydrate was added to the reaction mixture. The product was purified using silica gel chromatography, eluting with dichloromethane:methanol 90:10.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08420670B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-f2eb8e0e29f047f48370c0c6b573690f |
| Source note | uspto-grants-2013_04 |