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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1966532Generated: October 31, 2026

Benzenemethanamine, 3,4-dichloro- → HCID 59474745, compound

https://huagongshe.com/reaction/1966532

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzenemethanamine, 3,4-dichloro-HCID 1608—
ReactantHCID 43668467HCID 43668467—
CatalystCupric sulfate monohydrateHCID 61499—
ProductHCID 59474745HCID 59474745—

Reaction Steps

Preparation was made using a similar procedure as described in example 5, method 5.1. Starting materials were 4-chloro-2-methyl-8-propoxyquinoline and 3,4-dichlorobenzylamine. A catalytic effective amount of copper(II)sulphate hydrate was added to the reaction mixture. The product was purified using silica gel chromatography, eluting with dichloromethane:methanol 90:10.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08420670B2
Source datasetuspto-grants-2013_04
ORD IDord-f2eb8e0e29f047f48370c0c6b573690f
Source noteuspto-grants-2013_04