HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57516788, compound → HCID 57516787, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57516788 | HCID 57516788 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57516787 | HCID 57516787 | 60% |
Reaction Steps
(2-Dibenzylamino-1,1-dimethyl-ethoxy)-acetic acid ethyl ester (Example 172, step 1) was hydrogenated in EtOH with Pd(OH)2 for 16 hours at 60° C. The desired 6,6-dimethyl-morpholin-3-one (585 mg, 60% purity, quant.) was obtained as a colorless liquid, MS: m/e=129 (M+H+) and used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08420661B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-fb65578b63a646bba6117bdd89271d8c |
| Source note | uspto-grants-2013_04 |