HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4,4-difluoro-4-phenylbutanoate → Ethyl 4,4,5,5-tetrafluoro-6-(3-phenylpropoxy)hexanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4,4-difluoro-4-phenylbutanoate | HCID 67245996 | — |
| Reactant | Ethyl (2E)-4,4,5,5-tetrafluoro-6-{[(2E)-3-phenylprop-2-en-1-yl]oxy}-hex-2-enoate | HCID 86658309 | — |
| Product | Ethyl 4,4,5,5-tetrafluoro-6-(3-phenylpropoxy)hexanoate | HCID 86658312 | — |
Reaction Steps
Obtained from Intermediate 39 (1.2 g, 3.46 mmol) by the procedure described in Intermediate 21. Ethyl 4,4,5,5-tetrafluoro-6-(3-phenylpropoxy)hexanoate was obtained (1.0 g, 82%) as oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08420669B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-86aa78d0fce14300a4b36391ed36613d |
| Source note | uspto-grants-2013_04 |