HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59556890, compound → HCID 67105608, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59556890 | HCID 59556890 | — |
| Reactant | L-SELECTRIDE tetrahydrofuran | HCID 131725857 | — |
| Product | HCID 67105608 | HCID 67105608 | — |
Reaction Steps
Using 2-chloro-4-(5-isobutyl-3,3-dimethyl-2,4-dioxopyrrolidin-1-yl)benzonitrile (620 mg) and lithium tri(sec-butyl)borohydride-THF solution (2.92 mL, 1 mol/L), and in the same manner as in Example 5, the title compound was obtained as a colorless solid (yield: 363 mg, 58%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08420694B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-bd31596568e342249e2550b90916492a |
| Source note | uspto-grants-2013_04 |