HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59556993, compound → HCID 67105806, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59556993 | HCID 59556993 | — |
| Reactant | L-SELECTRIDE tetrahydrofuran | HCID 131725857 | — |
| Product | HCID 67105806 | HCID 67105806 | — |
Reaction Steps
Using 2-fluoro-3-methyl-4-(3,3,5-trimethyl-2,4-dioxopyrrolidin-1-yl)benzonitrile (60 mg) and lithium tri(sec-butyl)borohydride-THF solution (0.33 mL, 1 mol/L), and in the same manner as in Example 5, the title compound was obtained as colorless crystals (yield: 41.4 mg, 69%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08420694B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-838a76ec587144a090ddbb795c27d926 |
| Source note | uspto-grants-2013_04 |