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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1967632Generated: November 1, 2026

1,1,1-Trifluoro-2-iodoethane → HCID 178431472, compound

https://huagongshe.com/reaction/1967632

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,1,1-Trifluoro-2-iodoethaneHCID 67709—
ReactantHCID 58433050HCID 58433050—
ProductHCID 178431472HCID 178431472—

Reaction Steps

The compound was synthesized starting from tert-butyl 5-(2-(2,3-difluorophenyl)-4-hydroxy-3-methyl-5-oxo-2H-pyrrol-1(5H)-yl)-1H-benzo[d]imidazole-1-carboxylate (0.441 g, 1 mmol), trifluoroiodoethane (0.15 ml, 1.5 mmol) and P1-tBu (1.38 ml, 1.5 mmol) according to the method described above and was further purified by semi-preparative HPLC.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08420828B2
Source datasetuspto-grants-2013_04
ORD IDord-346f8288e6464497ad23b07a88aaf3cb
Source noteuspto-grants-2013_04