HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1,1-Trifluoro-2-iodoethane → HCID 178431472, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1,1-Trifluoro-2-iodoethane | HCID 67709 | — |
| Reactant | HCID 58433050 | HCID 58433050 | — |
| Product | HCID 178431472 | HCID 178431472 | — |
Reaction Steps
The compound was synthesized starting from tert-butyl 5-(2-(2,3-difluorophenyl)-4-hydroxy-3-methyl-5-oxo-2H-pyrrol-1(5H)-yl)-1H-benzo[d]imidazole-1-carboxylate (0.441 g, 1 mmol), trifluoroiodoethane (0.15 ml, 1.5 mmol) and P1-tBu (1.38 ml, 1.5 mmol) according to the method described above and was further purified by semi-preparative HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08420828B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-346f8288e6464497ad23b07a88aaf3cb |
| Source note | uspto-grants-2013_04 |