Hexane → HCID 86668472, compound

HRID 1968168Notes

Reaction equation

C(O[CH2:5][CH3:6])(=O)C.Br[C:8]1[CH:13]=[CH:12][C:11]([C:14]2[C:15]3[C:20]([C:21]([C:28]4[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=4)=[C:22]4[C:27]=2[CH:26]=[CH:25][CH:24]=[CH:23]4)=[CH:19][CH:18]=[CH:17][CH:16]=3)=[CH:10][CH:9]=1.[CH3:34][CH2:35][CH2:36][CH2:37][CH2:38][CH3:39]>>[C:20]1([C:21]2[C:28]3[C:33]([C:14]([C:11]4[CH:12]=[CH:13][C:8]([C:36]5[CH:35]=[CH:34][C:39]([C:36]6([C:6]7[CH:5]=[CH:13][CH:8]=[CH:9][CH:10]=7)[C:35]7[CH:27]=[CH:14][CH:11]=[CH:12][C:34]=7[C:16]7[C:37]6=[CH:38][CH:39]=[CH:20][CH:15]=7)=[CH:38][CH:37]=5)=[CH:9][CH:10]=4)=[C:27]4[C:22]=2[CH:23]=[CH:24][CH:25]=[CH:26]4)=[CH:32][CH:31]=[CH:30][CH:29]=3)[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=1

Participants

Reactant 3

HCID 8058Hexane

HCID 8857Ethyl Acetate

HCID 221382759-(4-Bromophenyl)-10-phenylanthracene

Product 1

HCID 86668472HCID 86668472, compound

Procedure

The Rf value of the obtained pale yellow powder by silica gel thin layer chromatography (TLC) (with a developing solvent containing ethyl acetate and hexane in a 1:5 ratio) was 0.63, and that of 9-(4-bromophenyl)-10-phenylanthracene was 0.78.

Sources & evidence

ORD record: ord-0d0436b258f84e689091445742c1bf82
Source dataset: uspto-grants-2013_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08421346B2

Reaction notes

Loading…