Trifluoroacetic acid → HCID 178525660, compound

HRID 1968362Notes

Reaction equation

HRID 1968362 reaction equation
[NH:1]1[CH:5]=[N:4][CH:3]=[N:2]1.[F:6][C:7]([F:12])([F:11])[C:8]([OH:10])=[O:9]>O>[O-:10][C:8]([C:7]([F:12])([F:11])[F:6])=[O:9].[NH+:1]1[NH:2][CH:3]=[N:4][CH:5]=1

Participants

4

Reactant 2

HCID 6422Trifluoroacetic acidHCID 92571H-1,2,4-Triazole

Product 1

HCID 178525660HCID 178525660, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

1,2,4-Triazole (2.0 g, 28.96 mmol) was dissolved in 5 ml of distilled water. Trifluoroacetic acid (2.15 ml, 3.30 g, 28.96 mmol) was added via syringe at room temperature and the reaction was stirred at room temperature for 1 hour. The water was removed in vacuo with heating to approximately 90° C. for 4 hours.

Workup

  1. customThe water was removed in vacuo
  2. temperaturewith heating to approximately 90° C. for 4 hours

Sources & evidence

ORD record
ord-f78aa89593ee41fe95598d2a0db42f47
Source dataset
uspto-grants-2013_04
Patent number
US08425702B2

Reaction notes

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