Carbon Dioxide → HCID 131729145, compound

HRID 1968366Notes

Reaction equation

HRID 1968366 reaction equation
[C:1]([OH:5])(=[O:4])[CH2:2][OH:3].C(=O)(O)O.[NH2:10][C:11]([NH2:13])=[NH:12].C(=O)=O>O>[C:1]([O-:5])(=[O:4])[CH2:2][OH:3].[NH2:12][C:11]([NH2:13])=[NH2+:10]

Participants

5

Reactant 3

HCID 280Carbon DioxideHCID 757Glycolic AcidHCID 286947Carbonic acid-guanidine (1:1)

Product 1

HCID 131729145HCID 131729145, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Glycolic acid (3.0 g, 39.45 mmol) was dissolved in 15 ml of distilled water. Guanidine carbonate (3.55 g, 19.72 mmol) was added in portions at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 4 hours. The water was removed in vacuo with heating to approximately 90° C. The product was isolated as a white solid.

Workup

  1. customThe water was removed in vacuo
  2. temperaturewith heating to approximately 90° C
  3. customThe product was isolated as a white solid

Sources & evidence

ORD record
ord-5018a201eb4d485898ba05f6a69f32f0
Source dataset
uspto-grants-2013_04
Patent number
US08425702B2

Reaction notes

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