HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 23659326, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 3-Chloropyrazine-2-carbonitrile | HCID 292465 | — |
| Reactant | HCID 178443318 | HCID 178443318 | — |
| Solvent | Benzene | HCID 241 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 23659326 | HCID 23659326 | — |
Reaction Steps
The title compound was prepared according to Example 1 by using 5-(dodecylthio)-1,3,4-thiadiazole-2-thiol (319 mg, 1.00 mmol), NaH (60% dispersion in mineral oil, 44 mg, 1.10 mmol), and 3-chloropyrazine-2-carbonitrile (140 mg, 1.00 mmol) in DMF and benzene (6 ml, 1/1) by stirring at room temperature under nitrogen atmosphere overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426358B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-5cba523c3b8a458cb4573b18edf37f4d |
| Source note | uspto-grants-2013_04 |