HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178476501, compound → [3-(4-{1,2-Dimethyl-1-[5-(pyridin-2-ylmethoxy)pyridin-2-yl]propyl}phenyl)-1,2,4-oxadiazol-5-yl]methyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178476501 | HCID 178476501 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | [3-(4-{1,2-Dimethyl-1-[5-(pyridin-2-ylmethoxy)pyridin-2-yl]propyl}phenyl)-1,2,4-oxadiazol-5-yl]methyl acetate | HCID 57910807 | — |
Reaction Steps
A stirred solution of 3b (0.896 mmol) in xylene (6.00 mL) was heated to 110° C. for approximately 1 h. After cooling to rt, the reaction mixture was concentrated in vacuo to afford the title compound 3c, which was used without further purification in the subsequent reaction. m/z (ES) 473 (MH)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426413B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-1dc3a3bbb5fd4217b5febcd6a44f47e9 |
| Source note | uspto-grants-2013_04 |