HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminopyridinium → HCID 25151979, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminopyridinium | HCID 444229 | — |
| Reactant | HCID 58096340 | HCID 58096340 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 25151979 | HCID 25151979 | — |
Reaction Steps
3-Chloro-N-(5-(N-methyl-N-phenylsulfamoyl)-2-(methylamino)phenyl)propanamide (1 g, 0.0026 mol) and 4-aminopyridinium (0.73 g, 0.0078 mol) were boiled in anhydrous acetone (50 ml) for 50 h. The residue was filtered and subjected to crystallization from a 10:1 mixture of acetonitrile with ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426433B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-db5527cebb60461a88e7fd549604e727 |
| Source note | uspto-grants-2013_04 |