反应详情

Ethenesulfonic acid cyclohexyl-methyl-amide (0.0167 mol) was reacted with a mixture of methanol/ammonia (10 mL) in an autoclave for 16 hours at room temperature, and then the solvent was evaporated. The residue was purified by column chromatography (eluent: 90:10 CH2Cl2:(CH3OH:NH3)). The purest product fractions were collected and the solvent was evaporated to yield the title compound as a residue.

1. customthe solvent was evaporated
2. customThe residue was purified by column chromatography (eluent: 90:10 CH2Cl2:(CH3OH:NH3))
3. customThe purest product fractions were collected
4. customthe solvent was evaporated