HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia methanol → 2-amino-N-cyclohexyl-N-methylethanesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia methanol | HCID 21705897 | — |
| Reactant | N-cyclohexyl-N-methylethenesulfonamide | HCID 58625116 | — |
| Product | 2-amino-N-cyclohexyl-N-methylethanesulfonamide | HCID 43175916 | — |
Reaction Steps
Ethenesulfonic acid cyclohexyl-methyl-amide (0.0167 mol) was reacted with a mixture of methanol/ammonia (10 mL) in an autoclave for 16 hours at room temperature, and then the solvent was evaporated. The residue was purified by column chromatography (eluent: 90:10 CH2Cl2:(CH3OH:NH3)). The purest product fractions were collected and the solvent was evaporated to yield the title compound as a residue.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426429B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-29190851ef6e425c8443a79478759340 |
| Source note | uspto-grants-2013_04 |